8,8-二甲基-7-氧代壬酸合成路线 （共 5 条）
反应条件
potassium hydroxide; water in methanol Decarboxylation; hydrolysis; 6 h; Heating;
参考文献
Glatthar, Ralf; Giese, Bernd
Organic Letters, 2000 , vol. 2, # 15 p. 2315 - 2317
反应条件
1.1: 98 percent / conc. sulfuric acid / 5 h / 20 °C 2.1: sodium hydride / dimethylformamide / 0.5 h / 20 °C 2.2: 78 percent / dimethylformamide / 65 h / 20 °C 3.1: 99 percent / potassium hydroxide; water / methanol / 6 h / Heating View Scheme
参考文献
Organic Letters, , vol. 2, # 15 p. 2315 - 2317
反应条件
1.1: sodium hydride / dimethylformamide / 0.5 h / 20 °C 1.2: 78 percent / dimethylformamide / 65 h / 20 °C 2.1: 99 percent / potassium hydroxide; water / methanol / 6 h / Heating View Scheme
参考文献
Organic Letters, , vol. 2, # 15 p. 2315 - 2317
反应条件
Yield given. Multistep reaction;
参考文献
Jendralla, Heiner
Tetrahedron Letters, 1982 , vol. 23, # 36 p. 3657 - 3660
反应条件
1: 99 percent / SOCl2, trace DMF / 4 h / 30 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 36 p. 3657 - 3660
