tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine in tetrahydrofuran
T=50°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Safi, M.; Fahrang, R.; Sinou, D.
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 527 - 530
bis(p-nitrophenyl) phosphorazidate; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene
2 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mizuno, Masanori; Shioiri, Takayuki
Chemical Communications, 1997 , # 22 p. 2165 - 2166
bis(p-nitrophenyl) phosphorazidate; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene
0.5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mizuno, Masanori; Shioiri, Takayuki
Chemical Communications, 1997 , # 22 p. 2165 - 2166
bis(p-nitrophenyl) phosphorazidate; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene
2 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mizuno, Masanori; Shioiri, Takayuki
Chemical Communications, 1997 , # 22 p. 2165 - 2166
tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine in tetrahydrofuran
T=50°C; 2 h; further Pd catalyst; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Safi, M.; Fahrang, R.; Sinou, D.
Tetrahedron Letters, 1990 , vol. 31, # 4 p. 527 - 530
tetrakis(triphenylphosphine) palladium(0); trimethylsilylazide; tetrabutyl ammonium fluoride in tetrahydrofuran
1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;