N-{1-[1-(4-氯苯基)环丁基]-3-甲基丁基}-甲酰胺合成路线 (共 6 条)
反应条件
in formic acid T=160 - 180°C; Leuckart Amide Synthesis; 24.5 h;
参考文献
Reddy, G. Om; Sarma; Chandrasekhar; Babu, J. Moses; Prasad; Raju, C.M. Haricharan
Organic Process Research and Development, 1999 , vol. 3, # 6 p. 488 - 492
反应条件
1: toluene / 2 h / Heating 2: NaBH4 / methanol / 1 h / 0 - 25 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 13, # 2 p. 107 - 109
反应条件
1: 74 percent / KOH / diethyl ether; dimethylsulfoxide / 1 h / 20 - 25 °C 3: 30 percent / HCO2H / 17 h / 180 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 21 p. 2583 - 2589
反应条件
1: NaBH4 / methanol / 1 h / 0 - 25 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 13, # 2 p. 107 - 109
参考文献
Jeffery, James E.; Kerrigan, Frank; Miller, Thomas K.; Smith, Graham J.; Tometzki, Gerald B.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 21 p. 2583 - 2589
参考文献
Tetrahedron Asymmetry, , vol. 13, # 2 p. 107 - 109