4-甲基-2,7-二-叔-丁基硫杂卓合成路线 （共 6 条）
反应条件
in deuterated toluene T=130°C; 105 h;
参考文献
Yamamoto, Kagetoshi; Matsukawa, Atsuhito; Murata, Ichiro
Chemistry Letters, 1985 , p. 1119 - 1122
反应条件
lithium aluminium tetrahydride; tri-n-hexylphosphine
1.) CCl4, -20 deg C, 2.) RT; Yield given. Multistep reaction;
参考文献
Kohashi, Yasuji; Yamazaki, Shoko; Yamamoto, Kagetoshi; Murata, Ichiro
Heterocycles, 1982 , vol. 19, # 1 p. 202
反应条件
lithium aluminium tetrahydride in diethyl ether
Ambient temperature; Yield given;
参考文献
Yamamoto, Kagetoshi; Yamazaki, Shoko; Kohashi, Yasuji; Matsukawa, Atsuhito; Murata, Ichiro
Chemistry Letters, 1982 , p. 1843 - 1846
反应条件
1: 15 h / -78 °C
2: 40 percent / p-TsOH / benzene
3: DIBAH / hexane / -30 °C
4: trihexylphosphine, CCl4 / 0.08 h / -10 °C
5: LiAlH4 / diethyl ether / Ambient temperature
View Scheme
参考文献
Yamamoto, Kagetoshi; Yamazaki, Shoko; Kohashi, Yasuji; Matsukawa, Atsuhito; Murata, Ichiro
Chemistry Letters, 1982 , p. 1843 - 1846
反应条件
1: 40 percent / p-TsOH / benzene
2: DIBAH / hexane / -30 °C
3: trihexylphosphine, CCl4 / 0.08 h / -10 °C
4: LiAlH4 / diethyl ether / Ambient temperature
View Scheme
参考文献
Yamamoto, Kagetoshi; Yamazaki, Shoko; Kohashi, Yasuji; Matsukawa, Atsuhito; Murata, Ichiro
Chemistry Letters, 1982 , p. 1843 - 1846
反应条件
1: DIBAH / hexane / -30 °C
2: trihexylphosphine, CCl4 / 0.08 h / -10 °C
3: LiAlH4 / diethyl ether / Ambient temperature
View Scheme
参考文献
Yamamoto, Kagetoshi; Yamazaki, Shoko; Kohashi, Yasuji; Matsukawa, Atsuhito; Murata, Ichiro
Chemistry Letters, 1982 , p. 1843 - 1846
