1: 91 percent / pyridine / 0.08 h / 125 °C / microwave irradiation 2: [hydroxy(tosyloxy)iodo]benzene / CHCl3 / 0.2 h / 60 °C / microwave irradiation 3: 3.51 g / aq. NaOH / methanol; CHCl3 / 0.08 h / 50 °C / microwave irradiation 4: 78 percent / Et3N; PdCl2; PPh3 / CuI / dimethylformamide / 0.13 h / 80 °C / microwave irradiation 5: 88 percent / H2 / Pd/C / methanol; dioxane / 1 h / 20 °C 6: 85 percent / K2CO3 / acetone / 0.42 h / 45 °C 7: 89 percent / K2CO3 / acetone / 0.13 h / microwave irradiation 8: 74 percent / TsOH*H2O; acetic acid / toluene / 0.25 h / 117 °C / microwave irradiation 9: 91 percent / BCl3 / CH2Cl2 / 2.5 h / cooling 10: 72 percent / aq. NaOH / methanol; dioxane / 0.33 h / 25 °C View Scheme