1,1-双(二苯基膦)乙烯合成路线 （共 7 条）
反应条件
triethylamine; NiCl2((PPh3)P)2 in N,N-dimethyl-formamide T=120°C; 3 h;
参考文献
Shulyupin, Mstilsav O.; Chirkov, Evgeniy A.; Kazankova, Marina A.; Beletskaya, Irina P.
Synlett, 2005 , # 4 art. no. G46004ST, p. 658 - 660
反应条件
Si2Cl6 in benzene Heating;
参考文献
Goli; Grim
Tetrahedron Letters, 1991 , vol. 32, # 30 p. 3631 - 3634
反应条件
bis(acetylacetonate)nickel(II) in toluene T=120°C; 7 h;
参考文献
Synlett, , # 4 art. no. G46004ST, p. 658 - 660
反应条件
1: triphenylphosphine With lithium in tetrahydrofuran 2: [14C]-1,1-Dichloroethylene in tetrahydrofuran; benzene
参考文献
Awad, Ibrahim M. A.; Hassan, Fatma S. M.; Mohamed, Adila E.; Al-Hossainy, Ahmed F.
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 7 p. 1251 - 1266
反应条件
1: 1.) n-BuLi / 1.) benzene, hexane, 30 min, 2.) reflux, 4 h 2: 88 percent / Si2Cl6 / benzene / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 32, # 30 p. 3631 - 3634
反应条件
lithium 1) THF, 1 h, reflux, 2) THF, benzene; Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 117, # 7 p. 2322 - 2327
反应条件
in tetrahydrofuran
T=20°C; 0.5 h;
参考文献
Schmidbaur, Hubert; Herr, Rudolf; Riede, Juergen
Angewandte Chemie, 1984 , vol. 96, # 3 p. 237 - 238
