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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
84553-45-7
合成路线
（共 11 条）
84553-40-2
→
反应条件
84553-45-7
反应条件
t-BuOI Irradiation;
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
84553-45-7
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 72 percent / tert-butyl hypoiodite / Irradiation View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-29-3
→
反应条件
84553-45-7
反应条件
1: 81 percent / hydrobromic acid, acetic anhydride / 24 h / Heating 2: 100 percent / diethyl ether 3: 85 percent / sulfur tetrafluoride 4: 90 percent / potassium hydroxide / H2O; ethanol 5: 72 percent / tert-butyl hypoiodite / Irradiation View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-28-2
→
反应条件
84553-45-7
反应条件
1: 60 percent / potassium hydroxide / H2O / 48 h / Heating 2: 81 percent / hydrobromic acid, acetic anhydride / 24 h / Heating 3: 100 percent / diethyl ether 4: 85 percent / sulfur tetrafluoride 5: 90 percent / potassium hydroxide / H2O; ethanol 6: 72 percent / tert-butyl hypoiodite / Irradiation View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-31-7
→
反应条件
84553-45-7
反应条件
1: 85 percent / sulfur tetrafluoride 2: 90 percent / potassium hydroxide / H2O; ethanol 3: 72 percent / tert-butyl hypoiodite / Irradiation View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
17946-71-3
+
84553-45-7
→
反应条件
84010-89-9
反应条件
in tetrahydrofuran
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
17946-71-3
+
84553-45-7
→
反应条件
84010-89-9
+
78142-52-6
反应条件
in tetrahydrofuran T=0°C; other 1,4-dihalobicyclo<2.2.1>heptanes; other reagent, other solvents; Product distributionMechanism;
参考文献
Adcock, William; Gangodawila, Hemakanthi
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6040 - 6047
84553-45-7
→
反应条件
88888-25-9
反应条件
1: 38 percent / 96 h / Irradiation 2: 64 percent / conc. nitric acid / acetic anhydride View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
84553-45-7
→
反应条件
88888-26-0
反应条件
1: 38 percent / 96 h / Irradiation 2: 64 percent / conc. nitric acid / acetic anhydride 3: 57 percent / H2 / 5percent Pd/C / ethanol / 2585.7 Torr View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
84553-45-7
→
反应条件
84553-43-5
反应条件
iodine cloride in monofluoro-trichloromethane Ambient temperature;
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
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