N-(2-(苯甲酰氧基)乙基)-N,N-二甲基-3-(三甲基硅烷基L)-1-丙铵碘化物合成路线 （共 3 条）
反应条件
in diethyl ether
1.) 35-40 deg C, 4 h, 2.) ca. 20 deg C, 16 h;
参考文献
Lukevits, E.; Veveris, M. M.; Atare, Z. A.; Segal, I. D.; Khokhlova, L. N.; Kimenis, A. A.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 10 p. 764 - 768
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 10 p. 1204 - 1209
反应条件
1: 66 percent / Et3N / butan-1-ol / 22 h / Heating
2: 60 percent / Et3N / diethyl ether / 3 h / Heating
3: 58 percent / diethyl ether / 1.) 35-40 deg C, 4 h, 2.) ca. 20 deg C, 16 h
View Scheme
参考文献
Lukevits, E.; Veveris, M. M.; Atare, Z. A.; Segal, I. D.; Khokhlova, L. N.; Kimenis, A. A.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 10 p. 764 - 768
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 10 p. 1204 - 1209
反应条件
1: 60 percent / Et3N / diethyl ether / 3 h / Heating
2: 58 percent / diethyl ether / 1.) 35-40 deg C, 4 h, 2.) ca. 20 deg C, 16 h
View Scheme
参考文献
Lukevits, E.; Veveris, M. M.; Atare, Z. A.; Segal, I. D.; Khokhlova, L. N.; Kimenis, A. A.
Pharmaceutical Chemistry Journal, 1982 , vol. 16, # 10 p. 764 - 768
Khimiko-Farmatsevticheskii Zhurnal, 1982 , vol. 16, # 10 p. 1204 - 1209
