(E)-2-甲氧基-4-丙-1-烯基苯基异丁酸酯合成路线 (共 2 条)
反应条件
[{RuCl(μ-Cl)(η3:η3-(2,7-dimethylocta-2,6-diene-1,8-diyl))}2] in methanol
T=80°C; 4 h; Inert atmosphereSealed tube; diastereoselective reaction;
参考文献
Diaz-Alvarez, Alba E.; Crochet, Pascale; Cadierno, Victorio
Tetrahedron, 2012 , vol. 68, # 12 p. 2611 - 2620
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: [{RuCl(μ-Cl)(η3:η3-(2,7-dimethylocta-2,6-diene-1,8-diyl))}2] / methanol / 4 h / 80 °C / Inert atmosphere; Sealed tube
View Scheme
参考文献
Diaz-Alvarez, Alba E.; Crochet, Pascale; Cadierno, Victorio
Tetrahedron, 2012 , vol. 68, # 12 p. 2611 - 2620