3-chloro-benzenecarboperoxoic acid

2: 1.) TMEDA, n-butyllithium / 1.) hexane, 25 deg C, 6 h; 2.) ether, 25 deg C, 5 h 3: 99 percent / NBS / acetonitrile; H2O / 20 h / 25 °C 4: 90 percent / m-hloroperbenzoic acid / 2-methyl-propan-2-ol / 8 h / Heating View Scheme

1: 99 percent / NBS / acetonitrile; H2O / 20 h / 25 °C 2: 90 percent / m-hloroperbenzoic acid / 2-methyl-propan-2-ol / 8 h / Heating View Scheme

1: 1.) TMEDA, n-butyllithium / 1.) hexane, 25 deg C, 6 h; 2.) ether, 25 deg C, 5 h 2: 99 percent / NBS / acetonitrile; H2O / 20 h / 25 °C 3: 90 percent / m-hloroperbenzoic acid / 2-methyl-propan-2-ol / 8 h / Heating View Scheme