反应条件
1: 100 percent / DIBAL-H / toluene / 7 h / -40 °C
2: 82 percent / Et3N, 4-(dimethylamino)pyridine / CH2Cl2 / 2 h / 0 °C
3: 96 percent / triethylammonium fluoride / acetonitrile / 12 h / 60 °C
4: 30 percent / N-BuLi, Pd(DIPHOS)2, DIPHOS / tetrahydrofuran / 48 h / Heating; other alkoxides
View Scheme
参考文献
Stanton, Susan A.; Felman, Steven W.; Parkhurst, Carol S.; Godleski, Stephen A.
Journal of the American Chemical Society, 1983 , vol. 105, # 7 p. 1964 - 1969
