2-萘-1-基-1H-吡咯合成路线 （共 14 条）
反应条件
sodium methylate in tetrahydrofuran; methanol
T=25°C;
参考文献
Burghart, Armin; Kim, Heejin; Welch, Mike B.; Thoresen, Lars H.; Reibenspies, Joe; Burgess, Kevin; Bergstroem, Fredrik; Johansson, Lennart B.-A.
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 7813 - 7819
反应条件
[(tris(1-pyrazolyl)borate)Ru(P(phenyl)3)(CH3CN)2]PF6
T=100°C; 15 h;
参考文献
Odedra, Arjan; Wu, Chang-Jung; Pratap, Taduri Bhanu; Huang, Chun-Wei; Ran, Ying-Fen; Liu, Rai-Shung
Journal of the American Chemical Society, 2005 , vol. 127, # 10 p. 3406 - 3412
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane
T=-30 - 0°C; 2.5 h;
2: With acetic acid in tetrahydrofuran; hexane
参考文献
Tanguy, Chloe; Bertus, Philippe; Szymoniak, Jan; Larionov, Oleg V.; De Meijere, Armin
Synlett, 2006 , # 14 p. 2339 - 2341
反应条件
lithium hydroxide in dimethyl sulfoxide
T=90°C; P=9120 Torr; 3 h;
参考文献
Korostova, S. E.; Trofimov, B. A.; Sobenina, L. N.; Mikhaleva, A. I.; Sigalov, M. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 10 p. 1043 - 1045
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 10 p. 1351 - 1353
反应条件
1: 93 percent / aq. Na2CO3 / Pd(PPh3)4 / toluene; methanol / 18 h / 80 °C
2: 78 percent / NaOMe / tetrahydrofuran; methanol / 12 h / 25 °C
View Scheme
参考文献
Burghart, Armin; Kim, Heejin; Welch, Mike B.; Thoresen, Lars H.; Reibenspies, Joe; Burgess, Kevin; Bergstroem, Fredrik; Johansson, Lennart B.-A.
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 7813 - 7819
反应条件
1: 34 percent / Na2CO3, H2O / Pd(PPh3)4 / 1,2-dimethoxy-ethane / Heating
2: NaOMe / methanol / Ambient temperature
View Scheme
参考文献
Johnson, Christopher N.; Stemp, Geoffrey; Anand, Neel; Stephen, Susanna C.; Gallagher, Timothy
Synlett, 1998 , # 9 p. 1025 - 1027
反应条件
triethanolamine; Pearlman's catalist
T=100°C; 24 h; Sealed tube; regioselective reaction;
参考文献
Jafarpour, Farnaz; Rahiminejadan, Soraya; Hazrati, Hamideh
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 3109 - 3112
反应条件
1: 92 percent / 2.5M BuLi / hexane; tetrahydrofuran / 4 h / -78 °C
2: 58 percent / NaOH / ethanol / 12 h / 90 °C
View Scheme
参考文献
Katritzky; Li; Gordeev
Synthesis, 1994 , # 1 p. 93 - 96
反应条件
ammonium acetate in toluene
参考文献
Jones, David J.; Gibson, Vernon C.
Heterocycles, 2006 , vol. 68, # 6 p. 1121 - 1138
反应条件
1: DIBAL-H / toluene / 5 h / -78 °C
2: NH4OAc / toluene
View Scheme
参考文献
Jones, David J.; Gibson, Vernon C.
Heterocycles, 2006 , vol. 68, # 6 p. 1121 - 1138
