反应条件
1: hydrogenchloride / water; methanol / 1 °C / |Reflux 2: triethylamine / diethyl ether / 1 h 3: potassium iodide; potassium carbonate / acetone / 120 h / 20 °C 4: sodium hydroxide / water; methanol / 2 h / 20 - 50 °C 5: hydrogen; C63H78IrNOP(2+)*C32H12BF24(1-) / methanol / 12 h / 60 °C / 4560.31 Torr / |Autoclave View Scheme
参考文献
Song, Song; Zhu, Shou-Fei; Pu, Liu-Yang; Zhou, Qi-Lin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 6072 - 6075
Angew. Chem., 2013 , vol. 125, # 23 p. 6188 - 6191
