1,3-双[(2,2-二甲基-1,3-二恶烷-5-基)氧代]-2-丙醇合成路线 （共 3 条）
反应条件
potassium hydroxide; water; tetra-(n-butyl)ammonium iodide
T=60°C; 40 h;
参考文献
Nemoto, Hisao; Kamiya, Masaki; Minami, Yuki; Araki, Takaaki; Kawamura, Tomoyuki
Synlett, 2007 , # 13 p. 2091 - 2095
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide
T=20°C; 24 h;
参考文献
Nemoto, Hisao; Kamiya, Masaki; Nakamoto, Aki; Katagiri, Ayato; Yoshitomi, Kohsuke; Kawamura, Tomoyuki; Hattori, Hatsuhiko
Chemistry Letters, 2010 , vol. 39, # 8 p. 856 - 857
反应条件
1.1: boron trifluoride diethyl etherate / 20 h / 0 °C
2.1: sodium methylate / methanol / 24 h / 20 °C
2.2: Amberlyst 15.(TM). / 0.08 h
3.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 24 h / 20 °C
View Scheme
参考文献
Nemoto, Hisao; Kamiya, Masaki; Nakamoto, Aki; Katagiri, Ayato; Yoshitomi, Kohsuke; Kawamura, Tomoyuki; Hattori, Hatsuhiko
Chemistry Letters, 2010 , vol. 39, # 8 p. 856 - 857
