2,3-二氟-4-羟基偶氮苯合成路线 (共 2 条)
反应条件
1: aniline With hydrogenchloride; sodium nitrite in water T=0 - 5°C; 2: 2,3-Difluoro-phenol With sodium hydroxide in water 3: With hydrogenchloride more than 3 stages;
参考文献
Bayer Chemicals AG
Patent: EP1514865 A1, 2005 ;
Location in patent: Page/Page column 8; 9 ;
反应条件
hydrogen; palladium 10 on activated carbon in ethanol T=20°C; P=750.075 Torr; 18 h;
参考文献
Bayer Chemicals AG
Patent: EP1514865 A1, 2005 ;
Location in patent: Page/Page column 9 ;