1,3-二(4-吡啶甲基)脲合成路线 （共 7 条）
反应条件
sodium azide in water; acetone
T=-5°C; 0.166667 h;
参考文献
Kamiya; Miyahara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 1 p. 385 - 389
反应条件
sodium azide in water; acetone
T=-5°C; 0.166667 h;
参考文献
Kamiya; Miyahara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 1 p. 385 - 389
反应条件
triethylamine in dichloromethane
参考文献
Kane, John J.; Liao, Ruey-Fen; Lauher, Joseph W.; Fowler, Frank W.
Journal of the American Chemical Society, 1995 , vol. 117, # 48 p. 12003 - 12004
反应条件
in toluene
T=20 - 80°C;
参考文献
Troff, Ralf W.; Hovorka, Rainer; Weilandt, Torsten; Luetzen, Arne; Cetina, Mario; Nieger, Martin; Lentz, Dieter; Rissanen, Kari; Schalley, Christoph A.
Dalton Transactions, 2012 , vol. 41, # 27 p. 8410 - 8420
反应条件
in acetone
1 h; Heating;
参考文献
Kamiya; Yamaguchi; Miyahara; Miyata
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 12 p. 3226 - 3229
反应条件
in ethanol; water
0.5 h;
参考文献
Kamiya; Miyahara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 1 p. 385 - 389
反应条件
1: 82 percent / 0.17 h / 70 °C
2: 62 percent / H2O; ethanol / 0.5 h
View Scheme
参考文献
Kamiya; Miyahara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 1 p. 385 - 389
