2-乙氧基吡啶-3-硼酸频哪醇酯合成路线 (共 2 条)
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in dimethyl sulfoxide T=95°C; 6 h; Inert atmosphere;
参考文献
PFIZER LIMITED; STORER, Robert, Ian; SWAIN, Nigel, Alan
Patent: WO2013/93688 A1, 2013 ;
Location in patent: Page/Page column 44-45 ;
反应条件
1: sodium hydride / mineral oil; tetrahydrofuran / 3 h / 20 °C / |Inert atmosphere 2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 6 h / 95 °C / |Inert atmosphere View Scheme