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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
84863-77-4
合成路线
（共 14 条）
67-56-1
甲醇
+
24680-42-0
→
反应条件
84863-77-4
反应条件
sulfuric acid Heating;
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
24680-30-6
→
反应条件
84863-77-4
反应条件
1: 18-crown-6 / acetonitrile / 20 °C 2: KOH / ethanol; H2O / Heating 3: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
24680-29-3
→
反应条件
84863-77-4
反应条件
1: HMPA; thionyl chloride / tetrahydrofuran / 20 °C 2: 18-crown-6 / acetonitrile / 20 °C 3: KOH / ethanol; H2O / Heating 4: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
40133-14-0
5-(4-氯苯在)噻吩-2-羧酸
→
反应条件
84863-77-4
反应条件
1: 86 percent / H2SO4 / toluene / 7 h / Heating 2: LiAlH4 / diethyl ether / Heating 3: HMPA; thionyl chloride / tetrahydrofuran / 20 °C 4: 18-crown-6 / acetonitrile / 20 °C 5: KOH / ethanol; H2O / Heating 6: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
38401-71-7
5-(4-氯苯基)噻吩-2-甲醛
→
反应条件
84863-77-4
反应条件
1: 86 percent / NaOH; Ag2O / H2O / 20 - 50 °C 2: 86 percent / H2SO4 / toluene / 7 h / Heating 3: LiAlH4 / diethyl ether / Heating 4: HMPA; thionyl chloride / tetrahydrofuran / 20 °C 5: 18-crown-6 / acetonitrile / 20 °C 6: KOH / ethanol; H2O / Heating 7: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
40133-23-1
2-(4-氯苯基)噻吩
→
反应条件
84863-77-4
反应条件
1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 2: 86 percent / NaOH; Ag2O / H2O / 20 - 50 °C 3: 86 percent / H2SO4 / toluene / 7 h / Heating 4: LiAlH4 / diethyl ether / Heating 5: HMPA; thionyl chloride / tetrahydrofuran / 20 °C 6: 18-crown-6 / acetonitrile / 20 °C 7: KOH / ethanol; H2O / Heating 8: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
108-90-7
氯苯
→
反应条件
84863-77-4
反应条件
1.1: AlCl3 / CS2 / 2.5 h / 20 °C 2.1: dimethylformamide / 22 h / 5 °C 3.1: H2SO4 / methanol / 1 h / Heating 3.2: chloranil / benzene / 2 h / Heating 4.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 5.1: 86 percent / NaOH; Ag2O / H2O / 20 - 50 °C 6.1: 86 percent / H2SO4 / toluene / 7 h / Heating 7.1: LiAlH4 / diethyl ether / Heating 8.1: HMPA; thionyl chloride / tetrahydrofuran / 20 °C 9.1: 18-crown-6 / acetonitrile / 20 °C 10.1: KOH / ethanol; H2O / Heating 11.1: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
40877-09-6
4,4'-二氯苯丁酮
→
反应条件
84863-77-4
反应条件
1.1: dimethylformamide / 22 h / 5 °C 2.1: H2SO4 / methanol / 1 h / Heating 2.2: chloranil / benzene / 2 h / Heating 3.1: POCl3 / 1,2-dichloro-ethane / 17 h / Heating 4.1: 86 percent / NaOH; Ag2O / H2O / 20 - 50 °C 5.1: 86 percent / H2SO4 / toluene / 7 h / Heating 6.1: LiAlH4 / diethyl ether / Heating 7.1: HMPA; thionyl chloride / tetrahydrofuran / 20 °C 8.1: 18-crown-6 / acetonitrile / 20 °C 9.1: KOH / ethanol; H2O / Heating 10.1: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
24680-31-7
→
反应条件
84863-77-4
反应条件
1: KOH / ethanol; H2O / Heating 2: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
649569-56-2
5-(4-氯苯基)噻吩-2-羧酸甲酯
→
反应条件
84863-77-4
反应条件
1: LiAlH4 / diethyl ether / Heating 2: HMPA; thionyl chloride / tetrahydrofuran / 20 °C 3: 18-crown-6 / acetonitrile / 20 °C 4: KOH / ethanol; H2O / Heating 5: 67 percent / H2SO4 / Heating View Scheme
参考文献
Noguchi, Toshiya; Hasegawa, Masahiro; Tomisawa, Kazuyuki; Mitsukuchi, Morihiro
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4729 - 4742
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