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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
848782-36-5
合成路线
（共 8 条）
918795-52-5
→
反应条件
848782-36-5
反应条件
trimethylsilyl iodide in N,N-dimethyl-formamide T=20°C;
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
66224-66-6
→
反应条件
848782-36-5
反应条件
1.1: 70 percent / dimethylformamide / 1 h / Heating 2.1: 38 percent / NaH / dimethylformamide / 16 h / 20 °C 3.1: 52 percent / sodium borohydride / methanol / 11 h / -5 - 0 °C 4.1: pyridine; DMAP / 48 h / 20 °C 5.1: 0.3 g / aq. NaOH / methanol / 48 h / 20 °C 6.1: ozone / methanol; H2O / -78 °C 6.2: 53 percent / sodium borohydride / methanol; H2O / -78 - 20 °C 7.1: 8 percent / dimethylformamide / 3.5 h / 20 - 50 °C 8.1: 38 percent / TMSI / dimethylformamide / 20 °C View Scheme
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
918795-57-0
→
反应条件
848782-36-5
反应条件
1: 75 percent / pyridine; DMAP / 48 h / 20 °C 2: 84 percent / triethylamine; DMAP / CH2Cl2 / 16 h / 20 °C 3: 18 percent / NaH / dimethylformamide / 4 h / 100 °C 4: 42 percent / NH3*H2O / methanol / 96 h / 20 °C 5: 38 percent / TMSI / dimethylformamide / 20 °C View Scheme
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
918795-56-9
→
反应条件
848782-36-5
反应条件
1: 36 percent / acetic acid / 16 h / 20 °C 2: 75 percent / pyridine; DMAP / 48 h / 20 °C 3: 84 percent / triethylamine; DMAP / CH2Cl2 / 16 h / 20 °C 4: 18 percent / NaH / dimethylformamide / 4 h / 100 °C 5: 42 percent / NH3*H2O / methanol / 96 h / 20 °C 6: 38 percent / TMSI / dimethylformamide / 20 °C View Scheme
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
918795-49-0
→
反应条件
848782-36-5
反应条件
1.1: ozone / methanol; H2O / -78 °C 1.2: 53 percent / sodium borohydride / methanol; H2O / -78 - 20 °C 2.1: 8 percent / dimethylformamide / 3.5 h / 20 - 50 °C 3.1: 38 percent / TMSI / dimethylformamide / 20 °C View Scheme
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
918795-60-5
→
反应条件
848782-36-5
反应条件
1: 84 percent / triethylamine; DMAP / CH2Cl2 / 16 h / 20 °C 2: 18 percent / NaH / dimethylformamide / 4 h / 100 °C 3: 42 percent / NH3*H2O / methanol / 96 h / 20 °C 4: 38 percent / TMSI / dimethylformamide / 20 °C View Scheme
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
918795-50-3
→
反应条件
848782-36-5
反应条件
1: 8 percent / dimethylformamide / 3.5 h / 20 - 50 °C 2: 38 percent / TMSI / dimethylformamide / 20 °C View Scheme
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
918795-62-7
→
反应条件
848782-36-5
反应条件
1: 18 percent / NaH / dimethylformamide / 4 h / 100 °C 2: 42 percent / NH3*H2O / methanol / 96 h / 20 °C 3: 38 percent / TMSI / dimethylformamide / 20 °C View Scheme
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
