3-(哌啶-1-磺酰基)苄胺合成路线 （共 3 条）
反应条件
hydrogen; palladium 10 on activated carbon in methanol
T=20°C; 23 h;
参考文献
Jitsuoka, Makoto; Nagase, Tsuyoshi; Sato, Nagaaki; Tsukahara, Daisuke
Patent: US2011/9622 A1, 2011 ;
Location in patent: Page/Page column 36 ;
反应条件
1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 4 h / 0 °C
1.2: 1 h / 0 °C
2.1: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 80 °C
3.1: sodium azide / N,N-dimethyl-formamide / 22 h / 20 °C
4.1: hydrogen / palladium 10 on activated carbon / methanol / 23 h / 20 °C
View Scheme
参考文献
Jitsuoka, Makoto; Nagase, Tsuyoshi; Sato, Nagaaki; Tsukahara, Daisuke
Patent: US2011/9622 A1, 2011 ;
反应条件
1: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 80 °C
2: sodium azide / N,N-dimethyl-formamide / 22 h / 20 °C
3: hydrogen / palladium 10 on activated carbon / methanol / 23 h / 20 °C
View Scheme
参考文献
Jitsuoka, Makoto; Nagase, Tsuyoshi; Sato, Nagaaki; Tsukahara, Daisuke
Patent: US2011/9622 A1, 2011 ;
