in acetone
Trimethylamine oxide is added to a soln. of the starting compd. in acetone and the mixt. is heated under reflux for 18 h.; The mixt. is evaporated under reduced pressure and chromd. on alumina (hexane).;
参考文献
Fornals, David; Pericas, Miquel A.; Serratosa, Felix; Vinaixa, Jordi; Font-Altaba, Manuel; Solans, Xavier
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2749 - 2752
Bou, Anna; Pericas, Miquel A.; Serratosa, Felix; Claret, Josep; Feliu, Joan Miquel; Muller, Carlos
Journal of the Chemical Society, Chemical Communications, 1982 , # 22 p. 1305 - 1306
