1,7-二氮杂双环[5.3.2]十二烷合成路线 （共 3 条）
反应条件
lithium aluminium tetrahydride in ethylene glycol dimethyl ether
24 h; Ambient temperature;
参考文献
Alder, Roger W.; Eastment, Paul; Moss, Richard E.; Sessions, Richard B.; Stringfellow, Martin A.
Tetrahedron Letters, 1982 , vol. 23, # 40 p. 4181 - 4184
反应条件
1: 74 percent / MgSO4 / CH2Cl2
2: 70 percent / LiAlH4 / 1,2-dimethoxy-ethane / 24 h / Ambient temperature
View Scheme
参考文献
Alder, Roger W.; Eastment, Paul; Moss, Richard E.; Sessions, Richard B.; Stringfellow, Martin A.
Tetrahedron Letters, 1982 , vol. 23, # 40 p. 4181 - 4184
反应条件
1: 74 percent / MgSO4 / CH2Cl2
2: 70 percent / LiAlH4 / 1,2-dimethoxy-ethane / 24 h / Ambient temperature
View Scheme
参考文献
Alder, Roger W.; Eastment, Paul; Moss, Richard E.; Sessions, Richard B.; Stringfellow, Martin A.
Tetrahedron Letters, 1982 , vol. 23, # 40 p. 4181 - 4184
