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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
849773-86-0
合成路线
（共 11 条）
849773-94-0
→
反应条件
849773-86-0
反应条件
hydrogen; palladium dihydroxide in N,N-dimethyl-formamide T=20°C; 6 h;
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
132131-24-9
2-氨基-5-碘苯甲腈
→
反应条件
849773-86-0
反应条件
1: 90 percent / sodium ethoxide / ethanol / 26 h / 80 - 150 °C 2: 45 percent / palladium(II) acetate; tri-o-tolyl phosphine; piperidine / dimethylformamide / 60 h / 120 °C 3: 70 percent / H2 / palladium(II) hydroxide / dimethylformamide / 24 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
132131-20-5
2,4-二氨基-6-碘喹唑啉
→
反应条件
849773-86-0
反应条件
1: 45 percent / palladium(II) acetate; tri-o-tolyl phosphine; piperidine / dimethylformamide / 60 h / 120 °C 2: 70 percent / H2 / palladium(II) hydroxide / dimethylformamide / 24 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
1885-29-6
2-氨基苯甲腈
→
反应条件
849773-86-0
反应条件
1: 88 percent / iodine monochloride; acetic acid / 5 h / 20 °C 2: 90 percent / sodium ethoxide / ethanol / 26 h / 80 - 150 °C 3: 45 percent / palladium(II) acetate; tri-o-tolyl phosphine; piperidine / dimethylformamide / 60 h / 120 °C 4: 70 percent / H2 / palladium(II) hydroxide / dimethylformamide / 24 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
340322-86-3
((4-(苄氧基)苯基)乙炔)三甲基硅烷
→
反应条件
849773-86-0
反应条件
1: 62 percent / potassium carbonate / methanol / 6 h / 20 °C 2: 45 percent / copper(I) iodide; palladium(II) acetate; tri-o-tolylphosphine / piperidine / dimethylformamide / 24 h / 90 °C 3: 50 percent / H2 / palladium(II) hydroxide / dimethylformamide / 6 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
4397-53-9
4-苄氧基苯甲醛
→
反应条件
849773-86-0
反应条件
1: 75 percent / potassium carbonate / dioxane; H2O / 48 h / Heating 2: 45 percent / palladium(II) acetate; tri-o-tolyl phosphine; piperidine / dimethylformamide / 60 h / 120 °C 3: 70 percent / H2 / palladium(II) hydroxide / dimethylformamide / 24 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
540-38-5
4-碘苯酚
→
反应条件
849773-86-0
反应条件
1: 92 percent / potassium carbonate / butan-2-one / 48 h / Heating 2: 94 percent / triethylamine; copper(I) iodide; bis(triphenylphosphine)palladium(II) chloride / 6 h / 20 °C 3: 62 percent / potassium carbonate / methanol / 6 h / 20 °C 4: 45 percent / copper(I) iodide; palladium(II) acetate; tri-o-tolylphosphine / piperidine / dimethylformamide / 24 h / 90 °C 5: 50 percent / H2 / palladium(II) hydroxide / dimethylformamide / 6 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
36438-64-9
→
反应条件
849773-86-0
反应条件
1: 45 percent / palladium(II) acetate; tri-o-tolyl phosphine; piperidine / dimethylformamide / 60 h / 120 °C 2: 70 percent / H2 / palladium(II) hydroxide / dimethylformamide / 24 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
19578-68-8
1-苄氧基-4-碘苯
→
反应条件
849773-86-0
反应条件
1: 94 percent / triethylamine; copper(I) iodide; bis(triphenylphosphine)palladium(II) chloride / 6 h / 20 °C 2: 62 percent / potassium carbonate / methanol / 6 h / 20 °C 3: 45 percent / copper(I) iodide; palladium(II) acetate; tri-o-tolylphosphine / piperidine / dimethylformamide / 24 h / 90 °C 4: 50 percent / H2 / palladium(II) hydroxide / dimethylformamide / 6 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
123-08-0
对羟基苯甲醛
→
反应条件
849773-86-0
反应条件
1: 75 percent / potassium carbonate / butan-2-one / 24 h / Heating 2: 75 percent / potassium carbonate / dioxane; H2O / 48 h / Heating 3: 45 percent / palladium(II) acetate; tri-o-tolyl phosphine; piperidine / dimethylformamide / 60 h / 120 °C 4: 70 percent / H2 / palladium(II) hydroxide / dimethylformamide / 24 h / 20 °C View Scheme
参考文献
Khabnadideh, Soghra; Pez, Didier; Musso, Alexander; Brun, Reto; Ruiz Perez, Luis M.; Gonzalez-Pacanowska, Dolores; Gilbert, Ian H.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2637 - 2649
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