4-(1-苯基乙基)间苯二酚合成路线 (共 7 条)
反应条件
1: With antimony trichloride in acetonitrile
T=65°C; 0.416667 h; Microwave irradiation;
2: With boron tribromide in dichloromethane
T=-20 - 0°C;
参考文献
Shukla, Prashant; Choudhary, Manoj K.; Nayak, Sandip K.
Synlett, 2011 , # 11 p. 1585 - 1591
反应条件
1: With antimony trichloride in acetonitrile
T=65°C; 0.416667 h; Microwave irradiation;
2: With boron tribromide in dichloromethane
T=-20 - 0°C;
参考文献
Shukla, Prashant; Choudhary, Manoj K.; Nayak, Sandip K.
Synlett, 2011 , # 11 p. 1585 - 1591
反应条件
1: With antimony trichloride in acetonitrile
T=65°C; 0.416667 h; Microwave irradiation;
2: With boron tribromide in dichloromethane
T=-20 - 0°C;
参考文献
Shukla, Prashant; Choudhary, Manoj K.; Nayak, Sandip K.
Synlett, 2011 , # 11 p. 1585 - 1591
反应条件
perchloric acid; acetic acid
参考文献
Deutsche Hydrierwerke
Patent: DE689600 , 1934 ;
DRP/DRBP Org.Chem.
反应条件
1: With antimony trichloride in acetonitrile
T=65°C; 25 h; Microwave irradiation;
2: With boron tribromide in dichloromethane
T=-20 - 0°C;
参考文献
Shukla, Prashant; Choudhary, Manoj K.; Nayak, Sandip K.
Synlett, 2011 , # 11 p. 1585 - 1591
反应条件
sulfonic acidic resin D072 in dichloromethane
Friedel-Crafts Alkylation; Reflux; Reagent/catalyst; regioselective reaction;
参考文献
Wen, Jingyun; Qi, Haofei; Kong, Xiangjin; Chen, Ligong; Yan, Xilong
Synthetic Communications, 2014 , vol. 44, # 13 p. 1893 - 1903
反应条件
aluminium phenoxide
T=140°C; 3 h;
参考文献
Kozlikovskii, Ya. B.; Koshchii, V. A.; Butov, S. A.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 543 - 546
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 3 p. 606 - 610