1,2,3,6-四氢邻苯二甲酰亚胺合成路线 （共 11 条）
反应条件
complexlt;3THF*Mg2Cl2O*TiNCOgt;6 in pyridine Heating; Yield given;
参考文献
Tetrahedron Letters, , vol. 28, # 49 p. 6187 - 6190
反应条件
T=100°C; Substitution; Thermolysis;
参考文献
Russian Journal of Organic Chemistry, , vol. 35, # 9 p. 1313 - 1317
反应条件
18-crown-6 ether; potassium carbonate in acetone 24 h; Ambient temperature;
参考文献
Ashkenazi, P.; Tatarsky, D.; Ginsburg, D.
Tetrahedron, 1984 , vol. 40, # 17 p. 3325 - 3328
反应条件
[Ru4H6(p-cumene)4]Cl2; hydrogen in water T=90°C; P=45003.6 Torr; 22 h;
参考文献
Aoun, Rimane; Renaud, Jean-Luc; Dixneuf, Pierre H.; Bruneau, Christian
Angewandte Chemie - International Edition, 2005 , vol. 44, # 13 p. 2021 - 2023
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 35 h; RefluxInert atmosphere;
参考文献
Anastasiadis, Charalampos; Hogarth, Graeme; Wilton-Ely, James D.E.T.
Inorganica Chimica Acta, 2010 , vol. 363, # 13 p. 3222 - 3228
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 21 h / 60 °C 2: dichloromethane / 21.5 h / 0 - 20 °C 3: sodium periodate; ruthenium(IV) oxide / acetonitrile; water; tetrachloromethane / 24 h / 20 °C 4: sodium acetate; acetic anhydride / 3 h / 120 °C View Scheme
参考文献
XI, Ning; WANG, Tingjin; YI, Lei
Patent: WO2013/138210 A1, 2013 ;
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 21 h / 60 °C
2: dichloromethane / 21.5 h / 0 - 20 °C
3: sodium periodate; ruthenium(IV) oxide / acetonitrile; water; tetrachloromethane / 24 h / 20 °C
4: sodium acetate; acetic anhydride / 3 h / 120 °C
5: sodium tetrahydroborate; ethanol / 4.5 h / 20 °C
View Scheme
参考文献
XI, Ning; WANG, Tingjin; YI, Lei
Patent: WO2013/138210 A1, 2013 ;
反应条件
1: 4-cyclohexene-1,2-dicarboximide With lithium aluminium tetrahydride in tetrahydrofuran
24 h; Heating;
2: di-tert-butyl dicarbonate in dichloromethane
1 h; Further stages.;
参考文献
Johnson, Timothy A.; Jang, Doo Ok; Slafer, Brian W.; Curtis, Michael D.; Beak, Peter
Journal of the American Chemical Society, 2002 , vol. 124, # 39 p. 11689 - 11698
反应条件
tetra-(n-butyl)ammonium iodide; potassium carbonate in acetone
T=40°C; 8 h;
参考文献
RANBAXY LABORATORIES LIMITED
Patent: WO2006/92710 A1, 2006 ;
Location in patent: Page/Page column 55 ;
反应条件
triethylamine in dichloro acid ethyl ester
参考文献
Laporte Industries Limited
Patent: US3993640 A1, 1976 ;
