反应条件
1: 55 percent / LiAlH4 / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) r. t. overnight 2: 90 percent / I2, P(red) / toluene / 8 h / Heating 3: 67 percent / KOH / methanol / 4 h / Heating 4: 76 percent / toluene / 12 h / 60 °C 5: 93 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / toluene / 24 h / Ambient temperature 6: 66 percent / DDQ / CH2Cl2 / 4 h / 0 °C View Scheme
参考文献
Groesbeek, M.; Galen, A. J. J. van; Ippel, J. H.; Berden, J. A.; Lugtenburg, J.
Recueil des Travaux Chimiques des Pays-Bas, 1993 , vol. 112, # 4 p. 237 - 246
