2-(4-氯苯甲酰)苯甲酸合成路线 (共 35 条)
反应条件
copper(l) iodide 1.) ether, -10 deg C, 2.) ether, -5 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 425, # 1-2 p. 201 - 208
反应条件
hydrazine hydrate in ethanol 5 h; Heating;
参考文献
Yamaguchi; Kamei; Koga; Akima; Kuroki; Ohi
Journal of Medicinal Chemistry, 1993 , vol. 36, # 25 p. 4052 - 4060
反应条件
1: sulfuric acid / 6 h / 135 °C 2: zinc; acetic acid; pyridine / 8 h / 110 °C View Scheme
参考文献
Srinivas; Arun Kumar; Srinivas, Kolupula; Bhanuprakash; Jayathirtha Rao
Journal of Structural Chemistry, 2012 , vol. 53, # 5 p. 851 - 865
Zh. Strukt. Kim., 2012 , vol. 53, # 5 p. 851 - 865,15
反应条件
hydrogenchloride; potassium hydroxide; hydroxylamine
参考文献
Buu-Hoi et al.
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 1083,1103
反应条件
formic acid; formamide T=140 - 150°C; 6 h;
参考文献
Kreher, Richard P.; Hennige, Hans; Konrad, Michael; Uhrig, Juergen; Clemens, Andrea
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1991 , vol. 46, # 6 p. 809 - 828
反应条件
1: sulfuric acid / 6 h / 135 °C 2: zinc; acetic acid; pyridine / 8 h / 110 °C 3: pyridine / 24 h / 220 °C 4: diisobutylaluminium hydride / 4 h / -78 °C View Scheme
参考文献
Srinivas; Arun Kumar; Srinivas, Kolupula; Bhanuprakash; Jayathirtha Rao
Journal of Structural Chemistry, 2012 , vol. 53, # 5 p. 851 - 865
Zh. Strukt. Kim., 2012 , vol. 53, # 5 p. 851 - 865,15
反应条件
1: calcium oxide; water / 325 °C 2: AlCl3 View Scheme
参考文献
Newton; Groggins
Industrial and Engineering Chemistry, 1935 , vol. 27, p. 1398
Chem. Zentralbl., 1936 , vol. 107, # I p. 4004
反应条件
sodium hydroxide T=200°C;
参考文献
Du Pont de Nemours and Co.
Patent: US2107652 , 1936 ;
Full Text Show Details
Newport Co.
Patent: DE545399 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 543
反应条件
1: calcium oxide; water / 325 °C 2: AlCl3 View Scheme
参考文献
Newton; Groggins
Industrial and Engineering Chemistry, 1935 , vol. 27, p. 1398
Chem. Zentralbl., 1936 , vol. 107, # I p. 4004
反应条件
sulfuric acid; nitric acid in water T=5 - 15°C; 1 h;
参考文献
ANGION BIOMEDICA CORP.
Patent: WO2006/36981 A2, 2006 ;
Location in patent: Page/Page column 83-84 ;