6-甲氧基-8-硝基喹啉合成路线 （共 32 条）
反应条件
1: <NH4>2S; ethanol
2: ethanol
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参考文献
Magidson et al.
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1936 , vol. 9, p. 304,314
Chem. Zentralbl., 1936 , vol. 107, # II p. 1543
反应条件
hydrogen; platinum(IV) oxide in ethyl acetate
P=1603.2 Torr; 1 h;
参考文献
Allahyari; Strother; Fraser; Verbiscar
Journal of Medicinal Chemistry, 1984 , vol. 27, # 3 p. 407 - 410
反应条件
hydrogen; platinum(IV) oxide
参考文献
Bolchoz, Laura J. C.; Budinsky, Robert A.; Mcmillan, David C.; Jollow, David J.
Journal of Pharmacology and Experimental Therapeutics, 2001 , vol. 297, # 2 p. 509 - 515
反应条件
sulfuric acid; water; nitric acid
参考文献
Topcijev
Doklady Akademii Nauk SSSR, 1935 , p. IV 201, 204
反应条件
1: sulfuryl chloride
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参考文献
Schultz et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 170
反应条件
1: With water; hydrogen bromide
16 h; Heating / reflux;
2: With sodium hydroxide; water
参考文献
METHYLGENE INC.
Patent: US2007/293530 A1, 2007 ;
Location in patent: Page/Page column 84 ;
US 20070293530 A1
参考文献
Schultz et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 170
参考文献
Schultz et al.
Journal of Organic Chemistry, 1946 , vol. 11, p. 170
反应条件
chloroform; water; bromine; calcium carbonate
anschliessend mit Cyclohexen und wss. Ammoniak;
参考文献
Tatsuoka et al.
Yakugaku Zasshi, 1949 , vol. 69, p. 33,35
Chem.Abstr., 1950 , p. 3496
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Elderfield et al.
Journal of Organic Chemistry, vol. 23, p. 1378
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Elderfield et al.
Journal of the American Chemical Society, vol. 77, p. 4819
反应条件
1: iron; calcium carbonate; chloroform; bromine / Reagens 4:Wasser, Erwaermen des Reaktionsprodukts mit einem Gemisch von Cyclohexen und Benzol
2: 130 - 140 °C / unter Druck
View Scheme
参考文献
Elderfield et al.
Journal of the American Chemical Society, vol. 77, p. 4819
