N,O-二叔丁氧羰基-羟胺合成路线 (共 16 条)
反应条件
hydroxylamine hydrochloride; triethylamine in water; Petroleum ether 1.) 0 deg C, 6 h, 2.) room temp., overnight;
参考文献
Baillie, Lynn C.; Batsanov, Andrei; Bearder, John R.; Whiting, Donald A.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 20 p. 3471 - 3478
反应条件
triethylamine in tert-butyl methyl ether; water; Petroleum ether
参考文献
WO2013/59194 A1, ;
Page/Page column 38 ;
反应条件
1: aqueous acetic acid; sodium nitrite 2: aq. NaOH solution View Scheme
参考文献
Journal of the American Chemical Society, , vol. 81, p. 955
反应条件
1: water; hydroxylamine hydrochloride / anschliessend mit wss. Natronlauge 2: aq. NaOH solution View Scheme
参考文献
Journal of the American Chemical Society, , vol. 81, p. 955
参考文献
Journal of the American Chemical Society, , vol. 81, p. 955
反应条件
triphenylphosphine; diethylazodicarboxylate in toluene T=-20°C; 1 h;
参考文献
Oehler, Elisabeth; Kanzler, Silvia
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 112, # 1-4 p. 71 - 90
反应条件
triphenylphosphine; diethylazodicarboxylate in toluene T=-20°C; 1.5 h;
参考文献
Oehler, Elisabeth; Kanzler, Silvia
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 112, # 1-4 p. 71 - 90
反应条件
triphenylphosphine; diethylazodicarboxylate in toluene T=-20°C; 4 h;
参考文献
Oehler, Elisabeth; Kanzler, Silvia
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 112, # 1-4 p. 71 - 90
反应条件
triphenylphosphine; diethylazodicarboxylate in toluene T=-20°C; 1.5 h;
参考文献
Oehler, Elisabeth; Kanzler, Silvia
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 112, # 1-4 p. 71 - 90
反应条件
triphenylphosphine; diethylazodicarboxylate in toluene T=-20°C; 1 h;
参考文献
Oehler, Elisabeth; Kanzler, Silvia
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 112, # 1-4 p. 71 - 90