n-butyllithium; potassium 2-methyl-2-butoxide 1) r.t., 16 h, 2) reflux, 6 h; further reagent: D2O; Mechanism;

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n-butyllithium; potassium 2-methyl-2-butoxide 1) hexane, 16 h, r.t.; 6 h, reflux, 2) hexane, -78 deg C; r.t., 20 h; Yield given. Multistep reaction;