反应条件
1.1: 90 percent / LiOH / 1,2-dimethoxy-ethane; H2O / 5 h / 23 °C 2.1: SOCl2; Et3N / CH2Cl2 / 2 h / 23 °C 3.1: TMSCl; pyridine / 0.17 h / 23 °C 3.2: 4-dimethylaminopyridine / CH2Cl2 / 16 h / 23 °C 4.1: tetrabutylammonium fluoride / dimethylsulfoxide / 50 °C View Scheme
参考文献
Varaprasad, Chamakura V.N.S.; Johnson, Francis
Tetrahedron Letters, 2005 , vol. 46, # 12 p. 2163 - 2165
