6-甲氧基-2-甲基-3-(甲基硫代)-1H-吡咯并[2,3-b]吡啶合成路线 (共 2 条)
反应条件
1: With tert-butylhypochlorite in dichloromethane
T=-78°C;
2: With triethylamine in dichloromethane
T=-78 - 20°C;
参考文献
Debenham, Sheryl D.; Chan, Audrey; Liu, Kun; Price, Karen; Wood, Harold B.
Tetrahedron Letters, 2005 , vol. 46, # 13 p. 2283 - 2285
反应条件
nickel in ethanol
T=20°C; 2.5 h;
参考文献
MERCK and CO., INC.
Patent: WO2009/5672 A1, 2009 ;
Location in patent: Page/Page column 66-67 ;