反应条件
1.1: 77 percent / N-bromosuccinimide; AIBN / benzene / 1 h / Heating
2.1: AcOH; K2CO3 / dimethylformamide / 2 h / 20 °C
2.2: 94 percent / KOH / dimethylformamide; methanol; H2O / 2 h / 20 °C
3.1: 86 percent / SmI2; HMPA / tetrahydrofuran / 2 h / 20 °C
4.1: 79 percent / Ag2CO3-Celite / benzene / 1.5 h / Heating
View Scheme
参考文献
Nishii, Yoshinori; Yoshida, Taichi; Asano, Hirofumi; Wakasugi, Kazunori; Morita, Jun-Ichi; Aso, Yoshifumi; Yoshida, Eri; Motoyoshiya, Jiro; Aoyama, Hiromu; Tanabe, Yoo
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2667 - 2678
