1.1: Et3N / CH2Cl2 / 4.5 h / 0 - 20 °C 2.1: 4.2 g / NaI / acetone / 16 h / Heating 3.1: 77 percent / acetonitrile / 16 h / Heating 4.1: KHMDS / tetrahydrofuran; CH2Cl2; toluene / 1.75 h / -78 - 20 °C 4.2: 51 percent / aq. HCl; ethyl acetate / tetrahydrofuran; CH2Cl2; toluene View Scheme
参考文献
Murphy, John A.; Commeureuc, Aurelien G. J.; Snaddon, Thomas N.; McGuire, Thomas M.; Khan, Tanweer A.; Hisler, Kevin; Dewis, Mark L.; Carling, Robert
Organic Letters, 2005 , vol. 7, # 7 p. 1427 - 1429
