6-溴-3-甲氧基-2-甲基吡啶合成路线 （共 4 条）
反应条件
potassium carbonate in acetone
16 h; Heating;
参考文献
Klumpp, Cedric; Burger, Alain; Mislin, Gaetan L.; Abdallah, Mohamed A.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 6 p. 1721 - 1724
反应条件
in methanol; dichloromethane
T=20°C;
参考文献
Klumpp, Cedric; Burger, Alain; Mislin, Gaetan L.; Abdallah, Mohamed A.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 6 p. 1721 - 1724
反应条件
1: 22 percent / Br2; aq. NaOH / 20 °C
2: 91 percent / methanol; CH2Cl2 / 20 °C
View Scheme
参考文献
Klumpp, Cedric; Burger, Alain; Mislin, Gaetan L.; Abdallah, Mohamed A.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 6 p. 1721 - 1724
反应条件
1: 84 percent / mCPBA / CHCl3 / 18 h / Heating
2: aq. NaOH / 0.33 h / 150 °C / 9000.72 Torr / microwave irradiation
View Scheme
参考文献
Klumpp, Cedric; Burger, Alain; Mislin, Gaetan L.; Abdallah, Mohamed A.
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 6 p. 1721 - 1724
