3-(丁基硫代)丙烷-1,2-二醇合成路线 （共 3 条）
反应条件
hydrogenchloride
T=50°C; 2 h;
参考文献
Etlis, V. S.; Shomina, F. N.; Tsareva, L. A.; Semenova, E. A.; Degtyareva, L. M.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 10 p. 1978 - 1982
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 10 p. 2194 - 2197
反应条件
sodium hydroxide in ethanol
4 h; Ambient temperature;
参考文献
Nabeshima, Tatsuya; Tsukada, Naoko; Haruyama, Tsutomu; Yano, Yumihiko
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 1 p. 227 - 229
反应条件
potassium hydroxide; acetic anhydride
1.) 130 deg C, 1 h, 2.) MeOH, 25 deg C to 30 deg C, 20 min; Multistep reaction;
参考文献
Kalugin, V. E.; Litvinov, V. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 7 p. 1391 - 1394
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 7 p. 1574 - 1578
