3-(4-硝基苄基)-3H-咪唑-4-甲醛合成路线 (共 5 条)
反应条件
in acetonitrile
T=60°C;
参考文献
Ohkanda; Lockman; Kothare; Qian; Blaskovich; Sebti; Hamilton
Journal of Medicinal Chemistry, 2002 , vol. 45, # 1 p. 177 - 188
反应条件
manganese(IV) oxide in 1,4-dioxane
8 h; Heating;
参考文献
Antonini, Ippolito; Cristalli, Gloria; Franchetti, Palmarisa; Grifantini, Mario; Martelli, Sante
Synthesis, 1983 , # 1 p. 47 - 49
反应条件
1: 30 percent / Na2CO3 / dimethylformamide / 18 h / 100 °C
2: 10 percent / activated MnO2 / dioxane / 8 h / Heating
View Scheme
参考文献
Antonini, Ippolito; Cristalli, Gloria; Franchetti, Palmarisa; Grifantini, Mario; Martelli, Sante
Synthesis, 1983 , # 1 p. 47 - 49
反应条件
1: 39 percent / NaNO2; HNO3 / 1 h / -10 °C
2: MnO2 / CHCl3 / Heating
View Scheme
参考文献
Zarghi; Derakhshandeh; Roshanzamir; Jorjani; Rastegar; Varmazyari; Shafiee
Bollettino Chimico Farmaceutico, 2002 , vol. 141, # 1 p. 15 - 20
反应条件
1: 85 percent / glacial acetic acid / butan-1-ol / 120 h
2: 39 percent / NaNO2; HNO3 / 1 h / -10 °C
3: MnO2 / CHCl3 / Heating
View Scheme
参考文献
Zarghi; Derakhshandeh; Roshanzamir; Jorjani; Rastegar; Varmazyari; Shafiee
Bollettino Chimico Farmaceutico, 2002 , vol. 141, # 1 p. 15 - 20