反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 0.33 h / Inert atmosphere
2: 1,8-diazabicyclo[5.4.0]undec-7-ene; 5-hydro-3-oxaoctafluoropentanesulfonyl fluoride / tetrahydrofuran / 0.08 h / Inert atmosphere
View Scheme
参考文献
Ding, Kai; Sun, Yun-Shan; Tian, Wei-Sheng
Journal of Organic Chemistry, 2011 , vol. 76, # 5 p. 1495 - 1498