(S)-5-吡咯烷-2-甲基-1H-四唑合成路线 （共 5 条）
反应条件
hydrogen; palladium on activated charcoal in water; acetic acid
P=760 Torr;
参考文献
Mitchell, Claire E. T.; Cobb, Alexander J. A.; Ley, Steven V.
Synlett, 2005 , # 4 art. no. D38604ST, p. 611 - 614
反应条件
1: pyridine / 20 °C
2: 93 percent / 50 °C
3: 73 percent / NaN3; NH4Cl / 150 °C
4: 55 percent / H2 / Pd/C / acetic acid; H2O / 760 Torr
View Scheme
参考文献
Mitchell, Claire E. T.; Cobb, Alexander J. A.; Ley, Steven V.
Synlett, 2005 , # 4 art. no. D38604ST, p. 611 - 614
反应条件
1: 93 percent / 50 °C
2: 73 percent / NaN3; NH4Cl / 150 °C
3: 55 percent / H2 / Pd/C / acetic acid; H2O / 760 Torr
View Scheme
参考文献
Mitchell, Claire E. T.; Cobb, Alexander J. A.; Ley, Steven V.
Synlett, 2005 , # 4 art. no. D38604ST, p. 611 - 614
反应条件
1: 73 percent / NaN3; NH4Cl / 150 °C
2: 55 percent / H2 / Pd/C / acetic acid; H2O / 760 Torr
View Scheme
参考文献
Mitchell, Claire E. T.; Cobb, Alexander J. A.; Ley, Steven V.
Synlett, 2005 , # 4 art. no. D38604ST, p. 611 - 614
反应条件
1: Et3N / CH2Cl2
2: pyridine / 20 °C
3: 93 percent / 50 °C
4: 73 percent / NaN3; NH4Cl / 150 °C
5: 55 percent / H2 / Pd/C / acetic acid; H2O / 760 Torr
View Scheme
参考文献
Mitchell, Claire E. T.; Cobb, Alexander J. A.; Ley, Steven V.
Synlett, 2005 , # 4 art. no. D38604ST, p. 611 - 614
