反应条件
1: methanol; (4S,2Z)-4-methyl-5-trityloxypent-2-ene With toluene-4-sulfonic acid T=20°C; 4 h; 2: (2S,3Z)-2-methylpent-3-ene-1-ol With oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-78°C; Swern oxidation; 0.583333 h; 3: With triethylamine in dichloromethane T=-78 - 0°C; 1.16667 h;
参考文献
Dunetz, Joshua R.; Julian, Lisa D.; Newcom, Jason S.; Roush, William R.
Journal of the American Chemical Society, 2008 , vol. 130, # 48 p. 16407 - 16416