反应条件
1: 76 percent / aq. KOH / acetonitrile; H2O / 3 h / 20 °C
2: 71 percent / aq. silver nitrate / acetonitrile; H2O / 16 h / 20 °C
3: 95 percent / Na; liq. NH3 / tetrahydrofuran / 0.5 h / -78 °C
4: 98 percent / Me3SiCl; NaI / acetonitrile / 24 h / 20 °C
5: 40 percent / t-BuOK / dimethylsulfoxide / 2 h / 50 °C
View Scheme
参考文献
Pauvert, Mickael; Collet, Sylvain; Guingant, Andre
Tetrahedron Letters, 2003 , vol. 44, # 22 p. 4203 - 4206
