乙基4-(2-氯-3-吡啶基)-4-氧代丁酸酯合成路线 （共 4 条）
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 6 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 3 p. 466 - 474
反应条件
1: With hydrogen; palladium on activated charcoal 2: With pyridinium chlorochromate
参考文献
Molecules, , vol. 9, # 6 p. 472 - 479
反应条件
1.1: LiHMDS / tetrahydrofuran / 0.25 h / -78 °C 1.2: 92 percent / tetrahydrofuran / 5 h / -78 °C 2.1: 48 percent / hydrogen / Pd/C / methanol / 5 h / atmospheric pressure 3.1: 67 percent / pyridinium chlorochromate / CH2Cl2 / 6 h / 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 3 p. 466 - 474
反应条件
1.1: LiHMDS / tetrahydrofuran / 0.25 h / -78 °C 1.2: 92 percent / tetrahydrofuran / 5 h / -78 °C 2.1: 48 percent / hydrogen / Pd/C / methanol / 5 h / atmospheric pressure 3.1: 67 percent / pyridinium chlorochromate / CH2Cl2 / 6 h / 20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 3 p. 466 - 474
