2-(4-异氰酰基苯基)噻吩合成路线 （共 3 条）
反应条件
1: Et3N, (PhO)2P(O)N3 / dimethylformamide / 37 °C
2: toluene / Heating
View Scheme
参考文献
Axton, Christopher A.; Billingham, Michael E. J.; Bishop, Paul M.; Gallagher, Peter T.; Hicks, Terence A.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 17 p. 2203 - 2214
反应条件
1: Na2CO3 / dioxane; H2O
2: Et3N, (PhO)2P(O)N3 / dimethylformamide / 37 °C
3: toluene / Heating
View Scheme
参考文献
Axton, Christopher A.; Billingham, Michael E. J.; Bishop, Paul M.; Gallagher, Peter T.; Hicks, Terence A.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 17 p. 2203 - 2214
反应条件
1: 85.49 percent / NaBF4, 4M HCl, NaNO2 / 0.33 h / 4 °C
2: 10 percent / KOAc / acetonitrile
3: Na2CO3 / dioxane; H2O
4: Et3N, (PhO)2P(O)N3 / dimethylformamide / 37 °C
5: toluene / Heating
View Scheme
参考文献
Axton, Christopher A.; Billingham, Michael E. J.; Bishop, Paul M.; Gallagher, Peter T.; Hicks, Terence A.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 17 p. 2203 - 2214
