反应条件
1.1: cyclohexene; palladium / methanol; ethyl acetate / 2 h / |Reflux; |Inert atmosphere 2.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -40 °C / |Inert atmosphere 2.2: -78 - 20 °C / |Inert atmosphere 3.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 20 °C / |Inert atmosphere View Scheme
参考文献
Moinizadeh, Nima; Klemme, Robby; Kansy, Marcus; Zimmer, Reinhold; Reissig, Hans-Ulrich
Synthesis (Germany), 2013 , vol. 45, # 19 art. no. SS-2013-T0413-OP, p. 2752 - 2762
