(3aR,6R,6aS)-6-羟基-2,2-二甲基二氢呋喃并[3,4-d][1,3]二氧杂环戊烯-4(3aH)-酮合成路线 (共 3 条)
反应条件
dimethylsulfide; ozone
1.) ethyl acetate, -78 deg C; 2.) 0 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Hudlicky, Tomas; Luna, Hector; Price, John D.; Rulin, Fan
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4683 - 4687
反应条件
sodium periodate; water
4 h; Ambient temperature;
参考文献
Mandel, Martin; Hudlicky, Tomas; Kwart, Lawrence D.
Collection of Czechoslovak Chemical Communications, 1993 , vol. 58, # 10 p. 2517 - 2522
反应条件
1: BuLi / CH2Cl2
2: LAH / diethyl ether
3: O3, DMS / CH2Cl2
View Scheme
参考文献
Hudlicky, Tomas; Luna, Hector; Price, John D.; Rulin, Fan
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4683 - 4687