(1S,5S,6S,7R,8S)-6,7,8-三羟基-1-(羟基甲基)-2-氧杂-4-氮杂双环[3.3.1]壬-3-酮合成路线 （共 6 条）
反应条件
barium dihydroxide in water T=70 - 80°C; 3 h;
参考文献
Horii, Satoshi; Fukase, Hiroshi; Kameda, Yukihiko
Carbohydrate Research, 1985 , vol. 140, p. 185 - 200
反应条件
sodium tetrahydroborate in water
2 h; Ambient temperature;
参考文献
Horii, Satoshi; Fukase, Hiroshi; Kameda, Yukihiko
Carbohydrate Research, 1985 , vol. 140, p. 185 - 200
反应条件
1: 12.5 g / H2O; dioxane / 18 h / Ambient temperature
2: 2.1 g / bromine / methanol / 1 h
3: 64 g / sodium borohydride / H2O / 2 h / Ambient temperature
View Scheme
参考文献
Horii, Satoshi; Fukase, Hiroshi; Kameda, Yukihiko
Carbohydrate Research, 1985 , vol. 140, p. 185 - 200
反应条件
1: 136 g / bromine / methanol / 1 h / 0 - 5 °C
2: 64 g / sodium borohydride / H2O / 2 h / Ambient temperature
View Scheme
参考文献
Horii, Satoshi; Fukase, Hiroshi; Kameda, Yukihiko
Carbohydrate Research, 1985 , vol. 140, p. 185 - 200
反应条件
sodium tetrahydroborate in water
2 h;
参考文献
Horii, Satoshi; Fukase, Hiroshi; Kameda, Yukihiko
Carbohydrate Research, 1985 , vol. 140, p. 185 - 200
反应条件
1: 2.1 g / bromine / methanol / 1 h
2: 64 g / sodium borohydride / H2O / 2 h / Ambient temperature
View Scheme
参考文献
Horii, Satoshi; Fukase, Hiroshi; Kameda, Yukihiko
Carbohydrate Research, 1985 , vol. 140, p. 185 - 200
