N-[3,5-双(三氟甲基)苯基]-N′-[(9R)-6′-甲氧基-9-金鸡宁]硫脲合成路线 （共 3 条）
反应条件
in tetrahydrofuran
T=20°C; 16 h;
参考文献
Berkessel, Albrecht; Mukherjee, Santanu; Mueller, Thomas N.; Cleemann, Felix; Roland, Katrin; Brandenburg, Marc; Neudoerfl, Joerg-M.; Lex, Johann
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 23 p. 4319 - 4330
反应条件
1.1: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 50 °C
2.1: triphenylphosphine / 15 h / 50 °C
2.2: 24 h / 20 °C
3.1: tetrahydrofuran / 20 °C
View Scheme
参考文献
Asano, Keisuke; Matsubara, Seijiro
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 16711 - 16713
反应条件
1.1: triphenylphosphine / 15 h / 50 °C
1.2: 24 h / 20 °C
2.1: tetrahydrofuran / 20 °C
View Scheme
参考文献
Asano, Keisuke; Matsubara, Seijiro
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 16711 - 16713
