4-(羟基甲基)-2,6-吡啶二甲酸2,6-二甲酯合成路线 （共 4 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C; 1.5 h;
参考文献
Tang, Rui-ren; Zhao, Qiang; Yan, Zi-er; Luo, Yi-ming
Synthetic Communications, 2006 , vol. 36, # 14 p. 2027 - 2034
反应条件
perchloric acid; Fe(ClO4)2·6H2O; dihydrogen peroxide in water
T=0 - 20°C; Fenton Reaction; 3 h; regioselective reaction;
参考文献
Kupai, Jozsef; Huszthy, Peter; Katz, Marianna; Toth, Tuende
Arkivoc, 2012 , vol. 2012, # 5 p. 134 - 145
反应条件
iron sulphate heptahydrate; sulfuric acid; dihydrogen peroxide in water
T=0 - 20°C;
参考文献
Labbe, Genevieve; Krismanich, Anthony P.; De Groot, Sarah; Rasmusson, Timothy; Shang, Muhong; Brown, Matthew D.R.; Dmitrienko, Gary I.; Guillemette, J. Guy
Journal of Inorganic Biochemistry, 2012 , vol. 112, p. 49 - 58
反应条件
1: CH3COCl
2: 41 percent / FeSO4*7H20; H2O2; H2SO4 / H2O / 15 - 30 °C
View Scheme
参考文献
Tang, Rui-ren; Zhao, Qiang; Yan, Zi-er; Luo, Yi-ming
Synthetic Communications, 2006 , vol. 36, # 14 p. 2027 - 2034
