2-(2,2-二氟乙氧基)乙醇合成路线 (共 2 条)
反应条件
1: 2,2-Difluoroethanol With tetrabutylammomium bromide; triethylamine
0.0833333 h;
2: 2-oxo-1,3-dioxolane T=110°C; 18 h;
参考文献
PFIZER LIMITED; PFIZER INC.
Patent: WO2005/49616 A1, 2005 ;
Location in patent: Page/Page column 146 ;
WO 2005/049616 A1
反应条件
1: 2,2-Difluoroethanol With tetrabutylammomium bromide; triethylamine
T=20°C; 0.0833333 h;
2: 2-oxo-1,3-dioxolane T=100°C; 18 h;
参考文献
THERACOS, INC.; SONG, Yanli
Patent: WO2009/26537 A1, 2009 ;
Location in patent: Page/Page column 78 ;