1: 98 percent / LiCl*H2O; water / dimethylsulfoxide / 16 h / 150 °C 2: 93 percent / LiOH*H2O / H2O; ethanol / 1 h 3: aq. NaOH; acylase I from Aspergillus melleus / CoCl2*6H2O / aq. phosphate buffer / 48 h / 39 °C / pH 7.2 View Scheme
参考文献
Kahnberg, Pia; Lucke, Andrew J.; Glenn, Matthew P.; Boyle, Glen M.; Tyndall, Joel D. A.; Parsons, Peter G.; Fairlie, David P.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7611 - 7622
1: 98 percent / LiCl*H2O; water / dimethylsulfoxide / 16 h / 150 °C 2: 93 percent / LiOH*H2O / H2O; ethanol / 1 h 3: aq. NaOH; acylase I from Aspergillus melleus / CoCl2*6H2O / aq. phosphate buffer / 48 h / 39 °C / pH 7.2 4: NaHCO3 / tetrahydrofuran / 2 h View Scheme
参考文献
Kahnberg, Pia; Lucke, Andrew J.; Glenn, Matthew P.; Boyle, Glen M.; Tyndall, Joel D. A.; Parsons, Peter G.; Fairlie, David P.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7611 - 7622
1: 98 percent / LiCl*H2O; water / dimethylsulfoxide / 16 h / 150 °C
2: 93 percent / LiOH*H2O / H2O; ethanol / 1 h
View Scheme
参考文献
Kahnberg, Pia; Lucke, Andrew J.; Glenn, Matthew P.; Boyle, Glen M.; Tyndall, Joel D. A.; Parsons, Peter G.; Fairlie, David P.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7611 - 7622
